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PinAAcle 900H Atomic Absorption Spectrometer

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PinAAcle 900H Atomic Absorption Spectrometer
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PinAAcle 900H Atomic Absorption Spectrometer

For laboratories needing a high-performance atomic absorption (AA) spectrometer, the PinAAcle 900H is a combined flame/furnace system with continuum source background correction.

Because different laboratories have different needs, we provide a full suite of powerful software tools for the PinAAcle 900H, starting with the innovative and easy-to-use Syngistix for AA Express, the more comprehensive Syngistix for AA standard software, or you can add on the special Syngistix Enhanced Security option that fulfills the special needs of highly regulated laboratories, such as those operating under the rules of 21 CFR Part 11.

Part Number PINAACLE900H

Overview

Through its ability to switch between flame and furnace in seconds, cutting-edge fiber optics to maximize light throughput for improved detection limits, high-speed automatic wavelength drive, automatic element identification with 8 lamp positions, the PinAAcle 900H can determine up to 20 elements in one completely automated run, maximizing your productivity.

The PinAAcle 900H is controlled by your choice of software packages:

  • Syngistix for AA Software: a workflow-based software designed to speed and simplify the journey from sample to results
  • Syngistix for AA Express Software: leverages the icon-based design of the Syngistix platform and delivers an even more streamlined workflow with only three steps to results

 

Specifications

21 CFR Part 11 Compatible Yes
Height 64.0 cm
Model Name PinAAcle 900H
Portable No
Product Brand Name PinAAcle
Warranty 1 Year
Weight 123.0 kg
Width 95.0 cm

Application Note

Analysis of Micronutrients in Fruit Juice Using FAST Flame Sample Automation for Increased Sample Throughput 

Consumers select fruit juice because it is a tasty, convenient beverage and generally understood to be a more nutritious alternative to carbonated beverages. For 100% juice products, the nutrition content of the original fruit itself is well known, which translates to the expected nutritional value of the final juice product. Detailed labeling is required on food products; for consumers, any comparative variance can be a strong incentive to choose one product over another. In an effort to appeal to consumers and address market needs, many juice products may also be fortified with micronutrients to boost or add to what is already present naturally.

While ICP-OES is generally favored as a multi-element analytical method, the cost savings, simplicity and speed of operation of flame atomic absorption (AA) provides an attractive alternative. This work demonstrates the ability of the PinAAcle 900 AA with a FAST Flame sample automation accessory to rapidly and accurately measure nutritional elements in fruit juices.

 

PDF 1 MB
Analysis of Micronutrients in Milk by Flame Atomic Absorption Using FAST Flame Sample Automation for Increased Sample Throughput 

Milk is an important source of nutrients, mainly for children. Because of its importance, milk is available in several different forms, most commonly as fresh, but it is also available in nonperishable forms (such as powdered and evaporated). Therefore, the requirement exists to analyze several forms of milk for nutritional elements. While ICP-OES is generally favored in a multi-element analytical environment, the cost savings, simplicity and speed of operation of a flame atomic absorption (AA) system provide an attractive alternative. Measuring multiple elements by flame AA requires each sample to be analyzed individually for each element, which impacts the speed advantage of flame AA – however, to address the speed issue, a fast, high-throughput sample automation system can be used.

This work demonstrates the ability of the PinAAcle 900 AA spectrometer to reliably and effectively analyze common nutritional elements in a variety of milks over a wide range of concentrations. Coupling the PinAAcle 900 with the FAST Flame 2 sample automation accessory minimizes user error when performing dilutions and making calibration standards increases throughput and provides excellent long-term stability, increasing productivity for the laboratory.

 

PDF 1 MB
Determination of Lead and Cadmium in Foods by Graphite Furnace Atomic Absorption Spectroscopy 

This work is focused on the use of GFAAS for the determination of lead and cadmium in a variety of food samples.The performance of this method was validated by assessing the Standard Reference Materials (SRMs) from the US National Institute of Standards and Technology (NIST) and China National Institute of Metrology (NIM) as well as by comparing these results with those obtained using inductively coupled plasma mass spectrometry (ICP-MS) after complete sample digestion by microwave method.

 

PDF 1 MB
Determination of Various Elements at Ultra-trace Levels in Ultrapure Acids and Photoresist Stripper Solutions by Graphite Furnace Atomic Absorption 

To protect the integrity of semiconductor and electronics end-products, semiconductor researchers and developers (R&D) and manufacturing QA/QC functions face unique challenges to reduce contaminates, sometimes down to ultra-trace levels. Metal determination in the sub-ppb range are required for the analysis of complex sample matrices and corrosive acids.

To meet these requirements, high-performance analytical techniques such as inductively coupled plasma mass spectrometry (ICP-MS) are preferred for rapid multi-element analysis, however, diagnosing problems can also involve only a few elements, in which graphite furnace atomic absorption spectrometry (GFAAS) is recommended.

Learn how GFAAS can help diagnose problems in semiconductor R&D and QA/QC processes.

 

PDF 1 MB
Direct Determination of Thallium in Water by Pre-concentration with PinAAcle 900H GFAAS 

Thallium is considered one of the most toxic heavy metals and a cumulative poison that can cause adverse health effects and degenerative changes in many organs. The main threat to humans is through occupational exposure and environmental contamination.

Industry’s use of thallium is widespread, and leaching from ore processing operations is the major source of elevated thallium concentrations in water. Due to thallium’s potential to cause adverse health effects in exposed people, a number of regulations and guidelines have been established by agencies around the world.

Graphite furnace atomic absorption spectrometry (GFAAS) has proven to be a well-established testing technique but is challenged with meeting the low detection limit requirements of the regulations by direct analysis, so the pre-concentration procedure is often needed. In this work, a PerkinElmer PinAAcle® 900H GFAA spectrometer combined with Syngistix for AA software were used to develop an accurate and reliable sample enrichment method for the determination of ultra-trace level thallium in water.

 

PDF 1 MB
Elemental Analysis of Beer by Flame Atomic Absorption with the PinAAcle 900This work demonstrates the ability to measure several elements in beer with Flame atomic absorption using the PinAAcle 900. No significant differences were observed between beers in glass bottles or metal cans.

PDF 953 KB
Fast Digestion Analysis of Lead and Cadmium in Rice Using GFAAS with Deuterium Background CorrectionToxic elements, such as lead (Pb) and cadmium (Cd), are entering the food chain through environmental contamination. Rice, as the most widely consumed cereal grain in Asia, can quickly pick up Pb and Cd from soil, thereby seriously endangering human health through diet. These toxic element levels need to be carefully monitored. Maximum levels of Pb and Cd are strictly regulated in Asian countries, especially in China; therefore, it is extremely important to develop a simple, reliable method for trace levels of Pb and Cd in rice. The allowable maximum levels of Pb and Cd in grains in EU and China are required to be below 0.2 mg/kg (Commission Regulation EC 1881/2006 and Chinese GB 2715-2016 Hygienic Standard). Graphite furnace atomic absorption spectroscopy (GFAAS) is the officially recommended technique for detection of trace elements in various food stuffs (GB/T 5009.15-2017, GB/T 5009. 12-2017 and EN 14083:2003). Food samples are usually pretreated before GFAAS analysis using various methods: microwave digestion, hot block digestion, dry ashing, and hot plate digestion. These conventional digestion procedures are usually complicated and time-consuming (2-4 hours or longer). Plus, they require large quantities of corrosive and oxidizing reagents, increasing the chance for contamination which could lead to inaccurate results. However, fast digestion can effectively speed up the sample preparation procedure while reducing the use of corrosive reagents and the chance for contamination.

PDF 912 KB
Micronutrients in Fortified Breakfast Cereal by Flame AA Using Microwave Digestion and FAST Flame Automation 

Fortified breakfast cereals are an important source of nutrition for children, and consumers have come to expect high quality from a variety of cereals and continue to select fortified products over non-fortified products in the marketplace. The efficient production of these nutritionally fortified breakfast cereals requires careful formulation and uniformity batch to batch. Ongoing analytical measurement of nutritional additives and the total micronutrient content in the cereal is one way in which food producers can quantify the quality and consistency of their cereal products.

While ICP-OES is generally favored as a multi-element analytical method, the cost savings, simplicity and speed of operation of flame atomic absorption (AA) provides an attractive alternative. This work demonstrates the ability of the PinAAcle 900 AA with a FAST Flame sample automation accessory to rapidly and accurately measure nutritional elements in a variety of fortified breakfast cereals.

 

PDF 1 MB
Micronutrients in Fresh and Dried Fruits by Flame AA Using Microwave Digestion and FAST Flame Automation 

With an increased focus on healthy living and the consumption of healthy foods, interest in the nutritional quality of the fruit we consume has become more important. When fresh fruit is not available, dried fruit is often substituted, and manufacturers and customers would like to know that the dried fruit has not lost some nutritional value during processing. One way of monitoring the quality of fresh or dried fruit is by measuring the micronutrient concentration contained within. Micronutrients are represented by trace elements considered to be nutritionally valuable, and it is these elements that can be analyzed via various inorganic analytical methods.

While ICP-OES is generally favored as a multi-element analytical method, the cost savings, simplicity and speed of operation of flame atomic absorption (AA) provides an attractive alternative. This work demonstrates the ability of the PinAAcle 900 AA spectrometer coupled to a FAST Flame sample automation accessory to analyze common nutritional elements in a variety of fresh and dried fruit.

 

PDF 1 MB
Quantification of Essential Metals in Spice Mixtures for Regulatory Compliance Using Flame Atomic Absorption SpectrophotometryThere is an increasing need to monitor the essential element levels in food samples at ever decreasing concentrations. For this purpose, very sensitive, yet rapid and inexpensive methods are necessary. The quantification of trace metals in food samples has routinely been carried out by ICP-OES, ICP-MS, graphite furnace atomic absorption (GFAA) and flame atomic absorption (FAA). Compared with other techniques, FAA has the characteristics of good precision and simplicity with lower cost and minimum operator proficiency.

PDF 993 KB
Simple and Reliable Determination of Heavy Metals in Soil with the PinAAcle 900H AA Spectrometer 

The heavy metal contamination of soil is one of the most widespread and severe environmental problems. This pollution not only decreases crop production, but also affects the health of people consuming the resulting food. With the increased knowledge about the impact of heavy metals from food on human health, the quality of soil resources has attracted considerable attention and concern.

Because they do not degrade and are toxic, heavy metals accumulate in the human body, leading to various serious diseases, including cancer. Cadmium (Cd), lead (Pb) and chromium (Cr) are commonly regarded as extremely toxic elements since they are harmful to humans, even at low concentrations. Zinc (Zn), nickel (Ni) and copper (Cu) are essential metals for plants at trace concentrations but are toxic if present at higher concentrations. Therefore, routine monitoring of these six metals in soil is vitally important to protect the quality and safety of food.

This work describes the analysis Cd, Cr, Cu, Pb, Ni, and Zn in soil using the PinAAcle 900H AA spectrometer, leveraging a rapid digestion procedure which uses less acid than conventional digestion methods.

 

PDF 2 MB
The Analysis of Copper, Iron, and Manganese in Wine with FAST Flame Atomic AbsorptionThis work demonstrates the ability of the PinAAcle 900 flame AA spectrometer to measure Cu, Fe, and Mn in wines to comply with Chinese wine import regulations coupled with FAST Flame sample automation for increased throughput.

PDF 747 KB
The Analysis of Major Elements in Drinking Water Using FAST Flame Sample Automation for Increased Sample ThroughputThis work demonstrates the analysis of mineral elements in a variety of drinking waters using the PinAAcle 900 AA spectrometer coupled with a FAST Flame accessory.

PDF 764 KB
The Determination of Minerals and Metals in Multi-Mineral/Multi-Vitamin Tablets by Flame Atomic Absorption SpectroscopyThere are many mineral dietary supplements available in today's marketplace to ensure that mineral deficiencies do not occur in one's diet. The mineral content of these products must be verified for quality control purposes.

PDF 427 KB
Trace Metals in Waters by GFAAS, in Accordance with U.S. EPA and Health Canada RequirementsPrecise and accurate measurements at the regulated levels are an important factor for assuring safe drinking water. U.S. EPA Method 200.91 is the method cited by EPA, Health Canada, and the WHO for the use of graphite furnace atomic absorption spectroscopy (GFAAS). In evaluating a GFAAS system for determination of these elements, it must provide good sensitivity, low noise, limited drift, and accuracy in matrices with high salt content (hard water) that might be found in drinking waters. In this work, the PinAAcle™ 900T, with a unique optical system, is evaluated for the use of EPA Method 200.9 for As, Cd, Pb, Se, and Tl in drinking waters.

PDF 289 KB

Brochure

Comprehensive Testing Solutions for Feed Millers 

Feed milling today is a complex business, and agribusinesses both large and small need to balance the nutritional and safety needs of livestock with availability of raw ingredients and their seasonality and variability. Add to that the valuable supplementation and medication that millers supply, and it’s clear: you’re creating a complete nutritional delivery system, not just a simple mix of grains.

 

PDF 3 MB
Grain Testing Solutions Brochure 

The grain industry is very complex. It’s global, diverse, and can also present analytical challenges. Today’s grain users demand more when it comes to quality, safety, and uniformity. In addition, they seek diverse products with unique characteristics.

PerkinElmer is equipped to help the grain industry in its quest to feed the world – nutritiously and economically. Our testing and analysis solutions encompass the three primary areas required for complete knowledge of grains and their derivatives – composition, functionality, and safety.

 

PDF 6 MB
Meat and Seafood Testing Solutions 

Food testing labs like yours are constantly challenged with accurately analyzing samples quickly and efficiently - all while striving to reduce costs due to market forces. Your commitment to ensuring meat and seafood are safe for consumption, as demand increases, is an uphill battle.

Our commitment to you: to provide a range of solutions across multiple technologies, products, and services that meets or exceeds the testing needs of food processors. Our solutions offer more efficiency and increased accuracy and sensitivity for better yields in real time with minimal training.

From instrumentation and software to consumables and reagents to service and support, we are dedicated to providing you with end-to-end solutions that ease your everyday challenges of automation, throughput, service, and time to results.

 

PDF 6 MB
PinAAcle 900 Series AA Spectrometers Brochure 

The PinAAcle series of atomic absorption (AA) spectrometers brings AA performance to new heights. Engineered with an array of exciting technological advances, it offers a variety of configurations and capabilities to deliver exactly the level of performance you need:

  • Flame only, furnace only, or space-saving stacked designs featuring both
  • Flame, furnace, flow injection, FIAS-furnace and mercury/hydride capabilities on a single instrument
  • Choice of Deuterium or longitudinal Zeeman background correction
  • TubeView color furnace camera simplifies autosampler tip alignment and sample dispensing
  • Syngistix for AA, a workflow-based software designed to speed and simplify the journey from sample to results

And no matter which model you select (900F, 900Z, 900H, 900T), you’ll discover an intuitive, highly efficient system capable of simplifying your journey from sample to results—even with the most difficult matrices. Experience peak performance and unmatched productivity. Step up to the PinAAcle series from PerkinElmer.

Download the brochure to learn more.

 

PDF 1 MB

Catalog

Atomic Spectroscopy 2018-2019 Consumables & Supplies CatalogWith instruments that are the industry standard worldwide, PerkinElmer accessories, consumables, methods and application support meet the most demanding requirements and are the preferred choice in thousands of laboratories globally.

PDF 8 MB

Flyer

High Quality and Performance in Atomic Absorption Grain Testing Ensemble Flyer 

Consumers are exposed to low levels of heavy metals on a daily basis and long term exposure can have negative health impacts. Since the elements themselves are distributed unevenly throughout, for example, cereal grain, with the germ and the outer layers having the highest concentrations, analyzing these grains to detect low analyte levels with accuracy and controlled reproducibility is a challenge.

The atomic absorption analysis technique provides a high performance option with features like a closed-furnace design that is sealed at both ends with easily removable bayonet-mount windows. In addition, independently controlled external and internal gas streams provide maximum flexibility, tube life, and sensitivity.

Systems like the PinAAcle 900 AA spectrometer make it faster and easier to get from sample to results by reducing your grain method development time, while PerkinElmer consumables and superior services will keep your lab at peak performance.

 

PDF 1 MB

Guide

Atomic Spectroscopy, A Guide to Selecting the Appropriate Technique and System 

Atomic spectroscopy is a family of techniques for determining the elemental composition of an analyte by its electromagnetic or mass spectrum. Several analytical techniques are available:

  • Atomic absorption (AA): flame and graphite furnace
  • Inductively coupled plasma optical emission spectroscopy (ICP-OES)
  • Inductively coupled plasma mass spectrometry (ICP-MS)

And selecting the most appropriate one is the key to achieving accurate, reliable, real-world results.

This guide provides a basic overview of the most commonly used techniques and the information necessary to help you select the one that best suits your specific needs and applications.

 

PDF 1 MB
PinAAcle 500/900 AA Spectrometers - Preparing Your LabThis document provides detailed instructions regarding the space, accessories and utilities required to operate PerkinElmer’s PinAAcle family of atomic absorption (AA) spectrometers (500 and 900 series) and other major AA accessories.

PDF 941 KB

Poster

Simple and Reliable Determination of Heavy Metals in Soil with the PinAAcle 900H AA SpectrometerA simple and rapid fast digestion technique followed by PinAAcle 900 AA analysis provides a new solution for determination of inorganic contaminants for a variety of soil samples.

PDF 334 KB

Product Note

Syngistix for AA Express Software - Only Three Steps to Reliable ResultsPerkinElmer’s Syngistix for AA Express software for the PinAAcle 900H AA spectrometer reduces complexity and speeds analysis time for an unmatched user experience.

PDF 1 MB

Regulatory Compliance Certification

Product Certificate - PinAAcle 900Product Certificate for the PinAAcle 900

PDF 614 KB

Technical Note

Analytical Quality with Genuine PerkinElmer Graphite PartsThe production of high-quality graphite components for atomic absorption spectroscopy requires stringent quality control. To ensure high quality and consistency, a specific high-density base graphite material has been developed for use with PerkinElmer graphite furnace systems.

PDF 245 KB

White Paper

The Determination of Metals in Non-Medical Face Masks 

With the onset of the COVID-19 pandemic, the use of face masks by the general public has become a critical personal protective measure to minimize person-to-person transmission. While health care workers use medical or surgical masks, the general population uses non-medical, otherwise known as hygienic, face masks to greatly reduce the transmission of SARS-CoV-2 by capturing droplets and aerosols from those infected with the virus.

In response to the increased demand for both the number and variety of non-medical face masks, many companies are now producing them to meet the public’s need, and with this great variety, the quality and the safety of the face masks must be assessed. This work describes the considerations surrounding metal analysis in hygienic face masks used to prevent the spread of COVID-19.

 

PDF 683 KB

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